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?:abstract
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A novel kind of magnetic porous carbon nano-fibers (Fe3O4@P-CNFs) materials was successfully prepared and used as an adsorbent. Based on the above-mentioned adsorbent, a simple and effective magnetic disperse solid-phase extraction (MSPE) method was developed and first utilized to the enrichment and purification of five Sudan dyes (including Sudan I, Sudan II, Sudan III, Sudan IV, and Sudan Red 7B) in foodstuffs for the first time. High-performance liquid chromatography was used to determine the content of the Sudan dyes. The parameters affecting the extraction performance were studied and optimized, including the amount of the adsorbent and inorganic salt, type and the volume of the eluent, pH of the sample solution and extraction time. Under the optimized experimental conditions, the results show that the proposed method has a good linear relationship (r≥ 0.9993). The limits of detection range from 0.88 µg L-1 to 1.27 µg L-1. The recoveries range from 86.6% to 99.7% with the relative standard deviations ranging from 0.6% to 7.9% in the methodology validation. The above-mentioned results indicate that the proposed method is a sensitive and reliable procedure with good reproducibility for the detection of Sudan dyes residues in foodstuffs.
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